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Year of publication
- 2021 (34) (remove)
Burning of clinker is the most influencing step of cement quality during the production process. Appropriate characterisation for quality control and decision-making is therefore the critical point to maintain a stable production but also for the development of alternative cements. Scanning electron microscopy (SEM) in combination with energy dispersive X-ray spectroscopy (EDX) delivers spatially resolved phase and chemical information for cement clinker. This data can be used to quantify phase fractions and chemical composition of identified phases.
The contribution aims to provide an overview of phase fraction quantification by semi-automatic phase segmentation using high-resolution backscattered electron (BSE) images and lower-resolved EDX element maps. Therefore, a tool for image analysis was developed that uses state-of-the-art algorithms for pixel-wise image segmentation and labelling in combination with a decision tree that allows searching for specific clinker phases. Results show that this tool can be applied to segment sub-micron scale clinker phases and to get a quantification of all phase fractions. In addition, statistical evaluation of the data is implemented within the tool to reveal whether the imaged area is representative for all clinker phases.
The development of a hydro-mechanically coupled Coupled-Eulerian–Lagrangian (CEL) method and its application to the back-analysisof vibratory pile driving model tests in water-saturated sand is presented. The predicted pile penetration using this approachis in good agreement with the results of the model tests as well as with fully Lagrangian simulations. In terms of pore water pressure, however, the results of the CEL simulation show a slightly worse accordance with the model tests compared to the Lagrangian simulation. Some shortcomings of the hydro-mechanically coupled CEL method in case of frictional contact problems and pore fluids with high bulk modulus are discussed. Lastly, the CEL method is applied to the simulation of vibratory driving of open-profile piles under partially drained conditions to study installation-induced changes in the soil state. It is concluded that the proposed method is capable of realistically reproducing the most important mechanisms in the soil during the driving process despite its addressed shortcomings.
The spread of breathing air when playing wind instruments and singing was investigated and visualized using two methods: (1) schlieren imaging with a schlieren mirror and (2) background-oriented schlieren (BOS). These methods visualize airflow by visualizing density gradients in transparent media. The playing of professional woodwind and brass instrument players, as well as professional classical trained singers were investigated to estimate the spread distances of the breathing air. For a better comparison and consistent measurement series, a single high note, a single low note, and an extract of a musical piece were investigated. Additionally, anemometry was used to determine the velocity of the spreading breathing air and the extent to which it was quantifiable. The results showed that the ejected airflow from the examined instruments and singers did not exceed a spreading range of 1.2 m into the room. However, differences in the various instruments have to be considered to assess properly the spread of the breathing air. The findings discussed below help to estimate the risk of cross-infection for wind instrument players and singers and to develop efficacious safety precautions, which is essential during critical health periods such as the current COVID-19 pandemic.
Biofeedback constitutes a well-established, non-invasive method to voluntary interfere in emotional processing by means of cognitive strategies. However, treatment durations exhibit strong inter-individual variations and first successes can often be achieved only after a large number of sessions. Sham feedback constitutes a rather untapped approach by providing feedback that does not correspond to the participant’s actual state. The current study aims to gain insights into mechanisms of sham feedback processing in order to support new techniques in biofeedback therapy. We carried out two experiments and applied different types of sham feedback on skin conductance responses and pupil size changes during affective processing. Results indicate that standardized but context-sensitive sham signals based on skin conductance responses exert a stronger influence on emotional regulation compared to individual sham feedback from ongoing pupil dynamics. Also, sham feedback should forego unnatural signal behavior to avoid irritation and skepticism among participants. Altogether, a reasonable combination of stimulus features and sham feedback characteristics enables to considerably reduce the actual bodily responsiveness already within a single session.
Besides their multiple known benefits regarding urban microclimate, living walls can be used as decentralized stand-alone systems to treat greywater locally at the buildings. While this offers numerous environmental advantages, it can have a considerable impact on the hygrothermal performance of the facade as such systems involve bringing large quantities of water onto the facade. As it is difficult to represent complex entities such as plants in the typical simulation tools used for heat and moisture transport, this study suggests a new approach to tackle this challenge by coupling two tools: ENVI-Met and Delphin. ENVI-Met was used to simulate the impact of the plants to determine the local environmental parameters at the living wall. Delphin, on the other hand, was used to conduct the hygrothermal simulations using the local parameters calculated by ENVI-Met. Four wall constructions were investigated in this study: an uninsulated brick wall, a precast concrete plate, a sandy limestone wall, and a double-shell wall. The results showed that the living wall improved the U-value, the exterior surface temperature, and the heat flux through the wall. Moreover, the living wall did not increase the risk of moisture in the wall during winter and eliminated the risk of condensation.
Entrepreneurship and start-up activities are seen as a key response to recent upheavals in the media industry: Newly founded ventures can act as important drivers for industry transformation and renewal, pioneering new products, business models, and organizational designs (e.g. Achtenhagen, 2017; Buschow & Laugemann, 2020).
In principle, media students represent a crucial population of nascent entrepreneurs: individuals who will likely become founders of start-ups (Casero-Ripollés et al., 2016). However, their willingness to start a new business is generally considered to be rather low (Goyanes, 2015), and for journalism students, the idea of innovation tends to be conservative, following traditional norms and professional standards (Singer & Broersma, 2020). In a sample of Spanish journalism students, López-Meri et al. (2020) found that one of the main barriers to entrepreneurial intentions is that students feel they lack knowledge and training in entrepreneurship.
In the last 10 years, a wide variety of entrepreneurship education courses have been set up in media departments of colleges and universities worldwide.
These programs have been designed to sensitize and prepare communications, media and journalism students to think and act entrepreneurially (e.g. Caplan et al., 2020; Ferrier, 2013; Ferrier & Mays, 2017; Hunter & Nel, 2011). Entrepreneurial competencies
and practices not only play a crucial role for start-ups, but, in imes of digital transformation, are increasingly sought after by legacy media companies as well (Küng, 2015).
At the Department of Journalism and Communication Research, Hanover University of Music, Drama and Media, Germany, we have been addressing these developments with the “Media Entrepreneurship” program. The course, established in 2013, aims to provide fundamental knowledge of entrepreneurship, as well as promoting students‘ entrepreneurial thinking and behavior. This article presents the pedagogical approach of the program and investigates learning outcomes. By outlining and evaluating the Media Entrepreneurship program, this article aims to promote good practices of entrepreneurship education in communications, media and journalism, and to reflect on the limitations of such programs.
According to Eurocode, the computation of bending strength for steel cantilever beams is a straightforward process. The approach is based on an Ayrton-Perry formula adaptation of buckling curves for steel members in compression, which involves the computation of an elastic critical buckling load for considering the instability. NCCI documents offer a simplified formula to determine the critical bending moment for cantilevers beams with symmetric cross-section. Besides the NCCI recommendations, other approaches, e.g. research literature or Finite-Element-Analysis, may be employed to determine critical buckling loads. However, in certain cases they render different results. Present paper summarizes and compares the abovementioned analytical and numerical approaches for determining critical loads and it exemplarily analyses corresponding cantilever beam capacities using numerical approaches based on plastic zones theory (GMNIA).
Scaling of concrete due to salt frost attack is an important durability issue in moderate and cold climates. The actual damage mechanism is still not completely understood. Two recent damage theories—the glue spall theory and the cryogenic suction theory—offer plausible, but conflicting explanations for the salt frost scaling mechanism. The present study deals with the cryogenic suction theory, which assumes that freezing concrete can take up unfrozen brine from a partly frozen deicing solution during salt frost attack. According to the model hypothesis, the resulting saturation of the concrete surface layer intensifies the ice formation in this layer and causes salt frost scaling. In this study an experimental technique was developed that makes it possible to quantify to which extent brine uptake can increase ice formation in hardened cement paste (used as a model material for concrete). The experiments were carried out with low temperature differential scanning calorimetry, where specimens were subjected to freeze–thaw cycles while being in contact with NaCl brine. Results showed that the ice content in the specimens increased with subsequent freeze–thaw cycles due to the brine uptake at temperatures below 0 °C. The ability of the hardened cement paste to bind chlorides from the absorbed brine at the same time affected the freezing/melting behavior of the pore solution and the magnitude of the ice content.
This study demonstrates the application and combination of multiple imaging techniques [light microscopy, micro-X-ray computer tomography (μ-CT), scanning electron microscopy (SEM) and focussed ion beam – nano-tomography (FIB-nT)] to the analysis of the microstructure of hydrated alite across multiple scales. However, by comparing findings with mercury intrusion porosimetry (MIP), it becomes obvious that the imaged 3D volumes and 2D images do not sufficiently overlap at certain scales to allow a continuous quantification of the pore size distribution (PSD). This can be overcome by improving the resolution and increasing the measured volume. Furthermore, results show that the fibrous morphology of calcium-silicate-hydrates (C-S-H) phases is preserved during FIB-nT. This is a requirement for characterisation of nano-scale porosity. Finally, it was proven that the combination of FIB-nT with energy-dispersive X-ray spectroscopy (EDX) data facilitates the phase segmentation of a 11 × 11 × 7.7 μm3 volume of hydrated alite.
Personalized ventilation (PV) is a mean of delivering conditioned outdoor air into the breathing zone of the occupants. This study aims to qualitatively investigate the personalized flows using two methods of visualization: (1) schlieren imaging using a large schlieren mirror and (2) thermography using an infrared camera. While the schlieren imaging was used to render the velocity and mass transport of the supplied flow, thermography was implemented to visualize the air temperature distribution induced by the PV. Both studies were conducted using a thermal manikin to simulate an occupant facing a PV outlet. As a reference, the flow supplied by an axial fan and a cased axial fan was visualized with the schlieren system as well and compared to the flow supplied by PV. Schlieren visualization results indicate that the steady, low-turbulence flow supplied by PV was able to penetrate the thermal convective boundary layer encasing the manikin's body, providing clean air for inhalation. Contrarily, the axial fan diffused the supplied air over a large target area with high turbulence intensity; it only disturbed the convective boundary layer rather than destroying it. The cased fan supplied a flow with a reduced target area which allowed supplying more air into the breathing zone compared to the fan. The results of thermography visualization showed that the supplied cool air from PV penetrated the corona-shaped thermal boundary layer. Furthermore, the supplied air cooled the surface temperature of the face, which indicates the large impact of PV on local thermal sensation and comfort.
Few studies have investigated how search behavior affects complex writing tasks. We analyze a dataset of 150 long essays whose authors searched the ClueWeb09 corpus for source material, while all querying, clicking, and writing activity was meticulously recorded. We model the effect of search and writing behavior on essay quality using path analysis. Since the boil-down and build-up writing strategies identified in previous research have been found to affect search behavior, we model each writing strategy separately. Our analysis shows that the search process contributes significantly to essay quality through both direct and mediated effects, while the author's writing strategy moderates this relationship. Our models explain 25–35% of the variation in essay quality through rather simple search and writing process characteristics alone, a fact that has implications on how search engines could personalize result pages for writing tasks. Authors' writing strategies and associated searching patterns differ, producing differences in essay quality. In a nutshell: essay quality improves if search and writing strategies harmonize—build-up writers benefit from focused, in-depth querying, while boil-down writers fare better with a broader and shallower querying strategy.
Marine macroalgae such as Ulva intestinalis have promising properties as feedstock for cosmetics and pharmaceuticals. However, since the quantity and quality of naturally grown algae vary widely, their exploitability is reduced – especially for producers in high-priced markets. Moreover, the expansion of marine or shore-based cultivation systems is unlikely in Europe, since promising sites either lie in fishing zones, recreational areas, or natural reserves. The aim was therefore to develop a closed photobioreactor system enabling full control of abiotic environmental parameters and an effective reconditioning of the cultivation medium in order to produce marine macroalgae at sites distant from the shore. To assess the feasibility and functionality of the chosen technological concept, a prototypal plant has been implemented in central Germany – a site distant from the sea. Using a newly developed, submersible LED light source, cultivation experiments with Ulva intestinalis led to growth rates of 7.72 ± 0.04 % day−1 in a cultivation cycle of 28 days. Based on the space demand of the production system, this results in fresh mass productivity of 3.0 kg m−2, respectively, of 1.1 kg m−2 per year. Also considering the ratio of biomass to energy input amounting to 2.76 g kWh−1, significant future improvements of the developed photobioreactor system should include the optimization of growth parameters, and the reduction of the system’s overall energy demand.
Carrier-bound titanium dioxide catalysts were used in a photocatalytic ozonation reactor for the degradation of micro-pollutants in real wastewater. A photocatalytic immersion rotary body reactor with a 36-cm disk diameter was used, and was irradiated using UV-A light-emitting diodes. The rotating disks were covered with catalysts based on stainless steel grids coated with titanium dioxide. The dosing of ozone was carried out through the liquid phase via an external enrichment and a supply system transverse to the flow direction. The influence of irradiation power and ozone dose on the degradation rate for photocatalytic ozonation was investigated. In addition, the performance of the individual processes photocatalysis and ozonation were studied. The degradation kinetics of the parent compounds were determined using liquid chromatography tandem mass spectrometry. First-order kinetics were determined for photocatalysis and photocatalytic ozonation. A maximum reaction rate of the reactor was determined, which could be achieved by both photocatalysis and photocatalytic ozonation. At a dosage of 0.4 mg /mg DOC, the maximum reaction rate could be achieved using 75% of the irradiation power used for sole photocatalysis, allowing increases in the energetic efficiency of photocatalytic wastewater treatment processes. The process of photocatalytic ozonation is suitable to remove a wide spectrum of micro-pollutants from wastewater.
Chemical glass frosting processes are widely used to create visual attractive glass surfaces. A commonly used frosting bath mainly contains ammonium bifluoride (NH4HF2) mixed with hydrochloric acid (HCl). The frosting process consists of several baths. Firstly, the preliminary bath to clean the object. Secondly, the frosting bath which etches the rough light scattering structure into the glass surface. Finally, the washing baths to clean the frosted object. This is where the constituents of the preceding steps accumulate and have to be filtered from the sewage. In the present contribution, phosphoric acid (H3PO4) was used as a substitute for HCl to reduce the amount of ammonium (NH4+) and chloride (Cl−) dissolved in the waste water. In combination with magnesium carbonate (MgCO3), it allows the precipitation of ammonium within the sewage as ammonium magnesium phosphate (MgNH4PO4). However, a trivial replacement of HCl by H3PO4 within the frosting process causes extensive frosting errors, such as inhomogeneous size distributions of the structures or domains that are not fully covered by these structures. By modifying the preliminary bath composition, it was possible to improve the frosting result considerably. To determine the optimal composition of the preliminary bath, a semi-automatic evaluation method has been developed. This method renders the objective comparison of the resulting surface quality possible.
Compiling and disseminating information about incidents and disasters are key to disaster management and relief. But due to inherent limitations of the acquisition process, the required information is often incomplete or missing altogether. To fill these gaps, citizen observations spread through social media are widely considered to be a promising source of relevant information, and many studies propose new methods to tap this resource. Yet, the overarching question of whether and under which circumstances social media can supply relevant information (both qualitatively and quantitatively) still remains unanswered. To shed some light on this question, we review 37 disaster and incident databases covering 27 incident types, compile a unified overview of the contained data and their collection processes, and identify the missing or incomplete information. The resulting data collection reveals six major use cases for social media analysis in incident data collection: (1) impact assessment and verification of model predictions, (2) narrative generation, (3) recruiting citizen volunteers, (4) supporting weakly institutionalized areas, (5) narrowing surveillance areas, and (6) reporting triggers for periodical surveillance. Furthermore, we discuss the benefits and shortcomings of using social media data for closing information gaps related to incidents and disasters.
The derivation of nonlocal strong forms for many physical problems remains cumbersome in traditional methods. In this paper, we apply the variational principle/weighted residual method based on nonlocal operator method for the derivation of nonlocal forms for elasticity, thin plate, gradient elasticity, electro-magneto-elasticity and phase-field fracture method. The nonlocal governing equations are expressed as an integral form on support and dual-support. The first example shows that the nonlocal elasticity has the same form as dual-horizon non-ordinary state-based peridynamics. The derivation is simple and general and it can convert efficiently many local physical models into their corresponding nonlocal forms. In addition, a criterion based on the instability of the nonlocal gradient is proposed for the fracture modelling in linear elasticity. Several numerical examples are presented to validate nonlocal elasticity and the nonlocal thin plate.
In this work, extensive reactive molecular dynamics simulations are conducted to analyze the nanopore creation by nano-particles impact over single-layer molybdenum disulfide (MoS2) with 1T and 2H phases. We also compare the results with graphene monolayer. In our simulations, nanosheets are exposed to a spherical rigid carbon projectile with high initial velocities ranging from 2 to 23 km/s. Results for three different structures are compared to examine the most critical factors in the perforation and resistance force during the impact. To analyze the perforation and impact resistance, kinetic energy and displacement time history of the projectile as well as perforation resistance force of the projectile are investigated.
Interestingly, although the elasticity module and tensile strength of the graphene are by almost five times higher than those of MoS2, the results demonstrate that 1T and 2H-MoS2 phases are more resistive to the impact loading and perforation than graphene. For the MoS2nanosheets, we realize that the 2H phase is more resistant to impact loading than the 1T counterpart.
Our reactive molecular dynamics results highlight that in addition to the strength and toughness, atomic structure is another crucial factor that can contribute substantially to impact resistance of 2D materials. The obtained results can be useful to guide the experimental setups for the nanopore creation in MoS2or other 2D lattices.
This article is focused on the research and development of new cellulose ether derivatives as innovative superplasticizers for mortar systems. Several synthetic strategies have been pursued to obtain new compounds to study their properties on cementitious systems as new bio-based additives. The new water-soluble admixtures were synthesized using a complex carboxymethylcellulose-based backbone that was first hydrolyzed and then sulfo-ethylated in the presence of sodium vinyl sulphonate. Starting with a complex biopolymer that is widely known as a thickening agent was very challenging. Only by varying the hydrolysis times and temperatures of the reactions was achieved the aimed goal. The obtained derivatives showed different molecular weight (Mw) and anionic charges on their backbones. An improvement in shear stress and dynamic viscosity values of CEM II 42.5R cement was observed with the samples obtained with a longer time of higher temperature hydrolysis and sulfo-ethylation. Investigations into the chemical nature of the pore solution, calorimetric studies and adsorption experiments clearly showed the ability of carboxymethyl cellulose superplasticizer (CMC SP) to interact with cement grains and influence hydration processes within a 48-h time window, causing a delay in hydration reactions in the samples. The fluidity of the cementitious matrices was ascertained through slump test and preliminary studies of mechanical and flexural strength of the hardened mortar formulated with the new ecological additives yielded values in terms of mechanical properties. Finally, the computed tomography (CT) images completed the investigation of the pore network structure of hardened specimens, highlighting their promising structure porosity.
Polylactic acid (PLA) is a highly applicable material that is used in 3D printers due to some significant features such as its deformation property and affordable cost. For improvement of the end-use quality, it is of significant importance to enhance the quality of fused filament fabrication (FFF)-printed objects in PLA. The purpose of this investigation was to boost toughness and to reduce the production cost of the FFF-printed tensile test samples with the desired part thickness. To remove the need for numerous and idle printing samples, the response surface method (RSM) was used. Statistical analysis was performed to deal with this concern by considering extruder temperature (ET), infill percentage (IP), and layer thickness (LT) as controlled factors. The artificial intelligence method of artificial neural network (ANN) and ANN-genetic algorithm (ANN-GA) were further developed to estimate the toughness, part thickness, and production-cost-dependent variables. Results were evaluated by correlation coefficient and RMSE values. According to the modeling results, ANN-GA as a hybrid machine learning (ML) technique could enhance the accuracy of modeling by about 7.5, 11.5, and 4.5% for toughness, part thickness, and production cost, respectively, in comparison with those for the single ANN method. On the other hand, the optimization results confirm that the optimized specimen is cost-effective and able to comparatively undergo deformation, which enables the usability of printed PLA objects.
Antimicrobial resistance (AMR) is identified by the World Health Organization (WHO) as one of the top ten threats to public health worldwide. In addition to public health, AMR also poses a major threat to food security and economic development. Current sanitation systems contribute to the emergence and spread of AMR and lack effective AMR mitigation measures. This study assesses source separation of blackwater as a mitigation measure against AMR. A source-separation-modified combined sanitation system with separate collection of blackwater and graywater is conceptually described. Measures taken at the source, such as the separate collection and discharge of material flows, were not considered so far on a load balance basis, i.e., they have not yet been evaluated for their effectiveness. The sanitation system described is compared with a combined system and a separate system regarding AMR emissions by means of simulation. AMR is represented in the simulation model by one proxy parameter each for antibiotics (sulfamethoxa-zole), antibiotic-resistant bacteria (extended-spectrum beta-lactamase E. Coli), and antibiotic re-sistance genes (blaTEM). The simulation results suggest that the source-separation-based sanitation system reduces emissions of antibiotic-resistant bacteria and antibiotic resistance genes into the aquatic environment by more than six logarithm steps compared to combined systems. Sulfa-methoxazole emissions can be reduced by 75.5% by keeping blackwater separate from graywater and treating it sufficiently. In summary, sanitation systems incorporating source separation are, to date, among the most effective means of preventing the emission of AMR into the aquatic envi-ronment.