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Year of publication
- 2015 (23) (remove)
Superplasticizers are utilized both to improve the fluidity during the placement and to reduce the water content of concretes. Both effects have also an impact on the properties of the hardened concrete. As a side effect the presence of superplasticizers affects the strength development of concretes that is strongly retarded. This may lead to an ecomomical drawback of the concrete manufacturing. The present work is aimed at gaining insights on the causes of the retarding effect of superplasticizers on the hydration of Portland cement. In order to simplify the complex interactions occurring during the hydration of Portland cement the majority of the work focuses on the interaction of superplasticizer and tricalcium silicate (Ca3SiO5 or C3S, the main compound of Portland cement clinker). The tests are performed in three main parts accompanied by methods as for example isothermal conduction calorimetry, electrical conductivity, Electron Microscopy, ICP-OES, TOC, as well as Analytical Ultracentrifugation.
In the first main part and based on the interaction of cations and anionic charges of polymers, the interactions between calcium ions and superplasticizers are investigated. As a main effect calcium ions are complexed by the functional groups of the polymers (carboxy, sulfonic). Calcium ions may be both dissolved in the aqueous phase and a constitute of particle interfaces. Besides these effects it is furthermore shown that superplasticizers induce the formation of nanoscaled particles which are dispersed in the aqueous phase (cluster formation). Analogous to recent findings in the field of biomineralization, it is reasonable to assume that these nanoparticles influence the crystal growth by their assembly process.
Based on the assumption that superplasticizers hinder either or both dissolution and precipitation and by that retard the cement hydration, the impact on separate reactions is investigated. On experiments that address the solubility of C-S-H phases and portlandite, it is shown that complexation of calcium ions in the aqueous phase by functional groups of polymers increases the solubility of portlandite. Contrary, in case of C-S-H solubility the complexation of calcium ions in solution leads to decrease of the calcium ion concentration in the aqueous phase. These effects are explained by differences in adsorption of polymers on C-S-H phases and portlandite. It is proposed that adsorption is stronger on C-S-H phases compared to portlandite due to the increased specific surface area of C-S-H phases. Following that, it is claimed that before polymers are able to adsorb on C-S-H phases the functional groups must be screened by calcium ions in the aqueous phase. It is further shown that data regarding the impact of superplasticizers on the unconstrained dissolution rate of C3S does not provide a clear relation to the overall retarding effect occurring during the hydration of C3S. Both increased and decreased dissolution rate with respect to the reference sample are detected. If the complexation capability of the superplasticizers is considered then also a reduced dissolution rate of C3S is determined. Despite the fact that the global hydration process is accelerated, the addition of calcite leads to a slower dissolution rate. Thus, a hindered unconstrained dissolution of C3S as possibly cause for the retarding effect still remains open for discussion. In the last section of this part, the pure crystallization of hydrate phases (C-S-H phases, portlandite) is fathomed. Results clearly show that superplasticizers prolong the induction time and modify the rate of crystal growth during pure crystallization in particular due to the complexation of ions in solution. But this effect is insufficient to account for the overall retarding effect. Further important factors are the blocking of crystal growth faces by adsorbed polymers and the dispersion of nanoscaled particles which hinders their agglomeration in order to build up crystals.
In the last main part of the work, the previously gathered results are utilized in order to investigate hydration kinetics. During hydration, dissolution and precipitation occur in parallel. Thereby, special attention is laid on the ion composition of the aqueous phase of C3S pastes and suspensions in order to determine the rate limiting step. All in all it is concluded that the retarding effect of superplasticizers on the hydration of tricalcium silicate is based on the retardation of crystallization of hydrate phases (C-S-H phases and portlandite). Thereby, the two effects complexation of calcium ions on surfaces and stabilization of nanoscaled particles are of major importance. These mechanisms may partly be compensated by template performance and increase in solubility by complexation of ions in solution. The decreased dissolution rate of C3S by the presence of superplasticizers during the in parallel occuring hydration process can only be assessed indirectly by means of the development of the ion concentrations in the aqueous phase (reaction path). Whether this observation is the cause or the consequence within the dissolution-precipitation process and therefore accounts for the retarding effect remains a topic for further investigations.
Besides these results it is shown that superplasticizers can be associated chemically with inhibitors because they reduce the frequency factor to end the induction period. Because the activation energy is widely unaffected it is shown that the basic reaction mechanism sustain. Furthermore, a method was developed which permits for the first time the determination of ion concentrations in the aqueous phase of C3S pastes in-situ. It is shown that during the C3S hydration the ion concentration in the aqueous phase is developed correspondingly to the heat release rate (calorimetry). The method permits the differentiation of the acceleration period in three stages. It is emphasized that crystallization of the product phases of C3S hydration, namely C-S-H phases and portlandite, are responsible for the end of the induction period.
One major research focus in the Material Science and Engineering Community in the past decade has been to obtain a more fundamental understanding on the phenomenon 'material failure'. Such an understanding is critical for engineers and scientists developing new materials with higher strength and toughness, developing robust designs against failure, or for those concerned with an accurate estimate of a component's design life. Defects like cracks and dislocations evolve at
nano scales and influence the macroscopic properties such as strength, toughness and ductility of a material. In engineering applications, the global response of the system is often governed by the behaviour at the smaller length scales. Hence, the sub-scale behaviour must be computed accurately for good predictions of the full scale behaviour.
Molecular Dynamics (MD) simulations promise to reveal the fundamental mechanics of material failure by modeling the atom to atom interactions. Since the atomistic dimensions are of the order of Angstroms ( A), approximately 85 billion atoms are required to model a 1 micro- m^3 volume of Copper. Therefore, pure atomistic models are prohibitively expensive with everyday engineering computations involving macroscopic cracks and shear bands, which are much larger than the atomistic length and time scales. To reduce the computational effort, multiscale methods are required, which are able to couple a continuum description of the structure with an atomistic description. In such paradigms, cracks and dislocations are explicitly modeled at the atomistic scale, whilst a self-consistent continuum model elsewhere.
Many multiscale methods for fracture are developed for "fictitious" materials based on "simple" potentials such as the Lennard-Jones potential. Moreover, multiscale methods for evolving cracks are rare. Efficient methods to coarse grain the fine scale defects are missing. However, the existing multiscale methods for fracture do not adaptively adjust the fine scale domain as the crack propagates. Most methods, therefore only "enlarge" the fine scale domain and therefore drastically increase computational cost. Adaptive adjustment requires the fine scale domain to be refined and coarsened. One of the major difficulties in multiscale methods for fracture is to up-scale fracture related material information from the fine scale to the coarse scale, in particular for complex crack problems. Most of the existing approaches therefore were applied to examples with comparatively few macroscopic cracks.
Key contributions
The bridging scale method is enhanced using the phantom node method so that cracks can be modeled at the coarse scale. To ensure self-consistency in the bulk, a virtual atom cluster is devised providing the response of the intact material at the coarse scale. A molecular statics model is employed in the fine scale where crack propagation is modeled by naturally breaking the bonds. The fine scale and coarse scale models are coupled by enforcing the displacement boundary conditions on the ghost atoms. An energy criterion is used to detect the crack tip location. Adaptive refinement and coarsening schemes are developed and implemented during the crack propagation. The results were observed to be in excellent agreement with the pure atomistic simulations. The developed multiscale method is one of the first adaptive multiscale method for fracture.
A robust and simple three dimensional coarse graining technique to convert a given atomistic region into an equivalent coarse region, in the context of multiscale fracture has been developed. The developed method is the first of its kind. The developed coarse graining technique can be applied to identify and upscale the defects like: cracks, dislocations and shear bands. The current method has been applied to estimate the equivalent coarse scale models of several complex fracture patterns arrived from the pure atomistic simulations. The upscaled fracture pattern agree well with the actual fracture pattern. The error in the potential energy of the pure atomistic and the coarse grained model was observed to be acceptable.
A first novel meshless adaptive multiscale method for fracture has been developed. The phantom node method is replaced by a meshless differential reproducing kernel particle method. The differential reproducing kernel particle method is comparatively more expensive but allows for a more "natural" coupling between the two scales due to the meshless interpolation functions. The higher order continuity is also beneficial. The centro symmetry parameter is used to detect the crack tip location. The developed multiscale method is employed to study the complex crack propagation. Results based on the meshless adaptive multiscale method were observed to be in excellent agreement with the pure atomistic simulations.
The developed multiscale methods are applied to study the fracture in practical materials like Graphene and Graphene on Silicon surface. The bond stretching and the bond reorientation were observed to be the net mechanisms of the crack growth in Graphene. The influence of time step on the crack propagation was studied using two different time steps. Pure atomistic simulations of fracture in Graphene on Silicon surface are presented. Details of the three dimensional multiscale method to study the fracture in Graphene on Silicon surface are discussed.
This thesis presents new interactive visualization techniques and systems intended to support users with real-world decisions such as selecting a product from a large variety of similar offerings, finding appropriate wording as a non-native speaker, and assessing an alleged case of plagiarism.
The Product Explorer is a significantly improved interactive Parallel Coordinates display for facilitating the product selection process in cases where many attributes and numerous alternatives have to be considered. A novel visual representation for categorical and ordered data with only few occurring values, the so-called extended areas, in combination with cubic curves for connecting the parallel axes, are crucial for providing an effective overview of the entire dataset and to facilitate the tracing of individual products. The visual query interface supports users in quickly narrowing down the product search to a small subset or even a single product. The scalability of the approach towards a large number of attributes and products is enhanced by the possibility of setting some constraints on final attributes and, therefore, reducing the number of considered attributes and data items. Furthermore, an attribute repository allows users to focus on the most important attributes at first and to bring in additional criteria for product selection later in the decision process. A user study confirmed that the Product Explorer is indeed an excellent tool for its intended purpose for casual users.
The Wordgraph is a layered graph visualization for the interactive exploration of search results for complex keywords-in-context queries. The system relies on the Netspeak web service and is designed to support non-native speakers in finding customary phrases. Uncertainties about the commonness of phrases are expressed with the help of wildcard-based queries. The visualization presents the alternatives for the wildcards in a multi-column layout: one column per wildcard with the other query fragments in between. The Wordgraph visualization displays the sorted results for all wildcards at once by appropriately arranging the words of each column. A user study confirmed that this is a significant advantage over simple textual result lists. Furthermore, visual interfaces to filter, navigate, and expand the graph allow interactive refinement and expansion of wildcard-containing queries.
Furthermore, this thesis presents an advanced visual analysis tool for assessing and presenting alleged cases of plagiarism and provides a three-level approach for exploring the so-called finding spots in their context. The overview shows the relationship of the entire suspicious document to the set of source documents. An intermediate glyph-based view reveals the structural and textual differences and similarities of a set of finding spots and their corresponding source text fragments. Eventually, the actual fragments of the finding spot can be shown in a side-by-side view with a novel structured wrapping of both the source, as well as the suspicious text. The three different levels of detail are tied together by versatile navigation and selection operations. Reviews with plagiarism experts confirm that this tool can effectively support their workflow and provides a significant improvement over existing static visualizations for assessing and presenting plagiarism cases.
The three main contributions of this research have a lot in common aside from being carefully designed and scientifically grounded solutions to real-world decision problems. The first two visualizations facilitate the decision for a single possibility out of many alternatives, whereas the latter ones deal with text at varying levels of detail. All visual representations are clearly structured based on horizontal and vertical layers contained in a single view and they all employ edges for depicting the most important relationships between attributes, words, or different levels of detail. A detailed analysis considering the context of the established decision-making literature reveals that important steps of common decision models are well-supported by the three visualization systems presented in this thesis.
This thesis deals with the basic design and rigorous analysis of cryptographic schemes and primitives, especially of authenticated encryption schemes, hash functions, and password-hashing schemes.
In the last decade, security issues such as the PS3 jailbreak demonstrate that common security notions are rather restrictive, and it seems that they do not model the real world adequately. As a result, in the first part of this work, we introduce a less restrictive security model that is closer to reality. In this model it turned out that existing (on-line) authenticated encryption schemes cannot longer beconsidered secure, i.e. they can guarantee neither data privacy nor data integrity. Therefore, we present two novel authenticated encryption scheme, namely COFFE and McOE, which are not only secure in the standard model but also reasonably secure in our generalized security model, i.e. both preserve full data inegrity. In addition, McOE preserves a resonable level of data privacy.
The second part of this thesis starts with proposing the hash function Twister-Pi, a revised version of the accepted SHA-3 candidate Twister. We not only fixed all known security issues
of Twister, but also increased the overall soundness of our hash-function design.
Furthermore, we present some fundamental groundwork in the area of password-hashing schemes. This research was mainly inspired by the medial omnipresence of password-leakage incidences. We show that the password-hashing scheme scrypt is vulnerable against cache-timing attacks due to the existence of a password-dependent memory-access pattern. Finally, we introduce Catena the first password-hashing scheme that is both memory-consuming and resistant against cache-timing attacks.
The main objective of this thesis is to investigate the characteristics of rice husk ash RHA) and then its behaviour in self-compacting high performance concrete (SCHPC) with respects to rheological properties, hydration and microstructure development and alkali silica reaction, in comparison with silica fume (SF). The main results show that the RHA is a macro-mesoporous amorphous siliceous material with a very high silica content comparable with SF. The pore size distribution is the most important parameter of RHA besides amorphous silica content. This parameter affects pore volume, specific surface area, and thus the water demand and the pozzolanic reactivity of RHA and its behaviour in SCHPC. The incorporation of RHA decreases filling and passing abilities, but significantly increases plastic viscosity and segregation resistance of SCHPC. Therefore, RHA can be used as a viscosity modifying admixture for SCHPC. The incorporation of RHA increases the superplasticizer adsorption, the superplasticizer saturation dosage, yield stress and plastic viscosity of mortar. Fresh mortar formulated from SCHPC is a shear-thickening material. The incorporation of RHA/SF ecreases the shearthickening degree. The incorporation of RHA/SF increases the degree of cement hydration. SF appears more effective at 3 days possibly due to the better nucleation site effect, whereas RHA dominates at the later ages possibly due to the internal water curing effect. The incorporation of RHA/SF increases the degree of C3S hydration, particularly the C3S hydration rate from 3 to 14 days. The pozzolanic reaction takes place outside and inside RHA particles.
The internal pozzolanic eaction products consolidate the pores inside RHA particles rather than contribute to the pore refinement in the cement matrix. In the presence of the high alkali concentration, RHA particles act as microreactive aggregates and react with alkali hydroxide to generate the expansive alkali silica reaction products. Increasing the particle size and temperature increases the alkali silica reactivity of RHA. The mechanism for the successive pozzolanic and alkali silica reactions of RHA is theorized. Additionally, a new simple
mix design method is proposed for SCHPC containing various supplementary cementitious materials, i.e. RHA, SF, fly ash and limestone powder.
Abstract
This doctoral thesis defines the relationship between the urban and rural in the 21st century, and focuses on food as a key component. The fact that food is, for the most part, produced in the countryside and then transported to the city has a significant influence on this very unbalanced relationship today. The main goal was to show that it is necessary to bring agriculture, urban gardening, the breeding of domestic farm animals, and beekeeping back to the city, which would have a positive affect on both the city and the countryside. All of this is already taking place at the local level, within the neighbourhoods of our cities and through the work of self-organised activities and initiatives, which have been taken up by city residents themselves. One example of this is the community garden, a new model of gardening which offers fertile ground for growing vegetables and to test various forms of co-existence, different ways of designing spaces, the creation of alternative values, and a positive vision for the future of city residents.
In 2010, I co-created the community urban garden Beyond a Construction Site, which is the central part of this artistic research. Throughout the entire four-year process of creating this community garden, theory and artistic practice were intertwined, and informed one another. This community garden is an example of a self-organised and self-managed community space located in a residential neighbourhood in the centre of the city of Ljubljana, and as such is a typical example of urbanism from the bottom up. I placed the creation and development of our community garden in a dialogue with the formal way of arranging urban gardening in Ljubljana, a top-down approach, which the city has been carrying out intensively since 2007. I compared the solutions being proposed by the city of Ljubljana for organising urban gardening with the way it is organised in other European cities, the UK, and the USA. I also researched the recent rapid growth of self-organised initiatives which are focused on the local production of food and seek to find more economic and ecologically friendly models to visibly influence the future of cities and the countryside. Here, community gardens play an important role, as in addition to the production of food they are also spaces for the criticism of existing urban policies, a self-organised revitalisation of neglected spaces, and places of resilience, because they differ from that which real estate agencies, large financial companies, and city authorities desire them to be.
The community garden Beyond a Construction Site has become living proof that, through a group action, the residents of a neighbourhood can influence existing city policies and the future of both their own neighbourhood and that of the entire city. The initiators of this garden are artists and architects, and we began this community garden in the context of an art festival, which also shows that art can influence the processes of everyday life and help to create much needed spaces within cities to serve various purposes. Our community garden has also shown itself to be an important platform for the exchange of knowledge on organic gardening, ecology in everyday life, and critical architecture, as well as serving to connect related initiatives. Together with these other initiatives we are stronger, and are influencing structural changes within city politics, thereby also co-creating the future of Ljubljana. This community garden is helping us to redefine our relationship with the city and re-awaken the desires and actions of residents connected with realising their fundamental right, the right to the city.
My other artworks, which I am presenting in the context of this doctoral thesis, show an optimistic vision for the future of cities. The video animations Back to the City (2011) and The Right Balance (2013), as well as the accompanying collages, visualise a city of the future where urban and rural practices live together side-by-side. This vision is being realised by city residents themselves, with their active participation in the creation of community gardens, growing their own vegetables, urban beekeeping, and by having egg-laying hens in their gardens. My desire was also to present the theoretical concept and scientific research to a non-academic public, and to people without specialised training. Using the method of storytelling I included knowledge from the research into the video animations and collages. In this way my artistic work, with an intentional playfulness, challenges today’s faith in science and theoretical concepts, as well as directing attention to working with common sense, with one’s own hands, and with the earth. This can contribute to a change in the still dominant anthropocentric view of nature, which is an urgently needed change for our future.
Keywords: rural, urban agriculture, community gardens, urban beekeeping, the bottom-up approach to urban planning, alternative spaces
Communities in discourse and space. Towards a spatial dialectic in gated residential developments
(2015)
This research projects deals with the discoursivity of spatial production.
By looking at contemporary residential development in the city of Istanbul, I will examine the reciprocity of the material production of space on one hand, and social discourses on the other, in order to make a contribution to how physical space can be used as a source of research in urban studies. In real estate marketing social discourses are used as a source of reference for place branding or identity design. Branding concepts therefore relate to how social groups imagine their position or future position in society, imaginaries that are continuously influenced and changed by social dynamics within the city but also from the outside. How such urban identities are formed and it what way they relate to the urban environment is crucial to a wide spectrum of social and cultural science. The constitutive role urban space attains has been described and analysed in much detail. Such scrutiny however has yet to be applied to the visual and communicative forms of engagement, the build environment partakes in the formation and change of social discourses.
In der vorliegenden Arbeit werden Manifestäußerungen des Design- und Architekturdiskurses im situativen, medialen, institutionellen und historischen Kontext untersucht. Auf Grundlage einer Analyse der Etymologie und der Ideengeschichte des Manifestes wird anhand ausgewählter Beispiele die These belegt, dass das Medium vor allem der gezielten Rezeptionssteuerung im Diskurs dient. Darüber hinaus wird die Fähigkeit und Bedeutung des Manifestes als Spiegel vergangener und gegenwärtiger, aber auch als Wegbereiter zukünftiger Diskurse analysiert und Entwicklungen des Manifestes hinsichtlich Stilistik, Inhalt, Funktion und Bedeutung im Design- und Architekturdiskurs dargestellt.
In der vorliegenden Arbeit werden Manifestäußerungen des Design- und Architekturdiskurses im situativen, medialen, institutionellen und historischen Kontext untersucht. Auf Grundlage einer Analyse der Etymologie und der Ideengeschichte des Manifestes wird anhand ausgewählter Beispiele die These belegt, dass das Medium vor allem der gezielten Rezeptionssteuerung im Diskurs dient. Darüber hinaus wird die Fähigkeit und Bedeutung des Manifestes als Spiegel vergangener und gegenwärtiger, aber auch als Wegbereiter zukünftiger Diskurse analysiert und Entwicklungen des Manifestes hinsichtlich Stilistik, Inhalt, Funktion und Bedeutung im Design- und Architekturdiskurs dargestellt.
Die Bau-Ausstellung zu Beginn des 20. Jahrhunderts oder „Die Schwierigkeit zu wohnen“, so lautet der Titel der Arbeit und legt damit ihren Fokus offen. Sie betrachtet ein um 1900 aufkommendes Ausstellungsphänomen in seinen ersten Dekaden; in einer Zeit, in der das Wohnen problematisiert wurde.
Der Praxis des Wohnens ist Anfang des 20. Jahrhunderts seine Selbstverständlichkeit abgesprochen worden. Die Bau-Ausstellung wird als ein Symptom dieses Verlusts interpretiert und zugleich als Versuch, ihm entgegenzuwirken. Statt sie innerdisziplinär als eine architekturgeschichtliche Episode der Moderne rein positivistisch zu beschreiben, legt die vorliegende Arbeit im Typus der Bau-Ausstellung eine weit reichende Problematik frei, die kulturphilosophische ebenso wie medientheoretische Dimensionen hat: Inwieweit lässt sich das Wohnen überhaupt ausstellen? Wie kann man eine alltägliche Praxis, die kaum eine Definition erlaubt, zeigen? Den Umgang mit dieser Aporie untersucht die Arbeit.